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And Huber, W. (2003) Electron Spin Resonance Spectroscopy of Organic Radicals. WileyVCH, Weinheim, Germany. 25. Moad, G. H. (1995) The Chemistry of Free Radical Polymerization. Pergamon, Bath. 26. A. P. (1972) Chemical Reviews, 72, 705. 27. , Sakai, M. and Miyaura, N. (1998) Journal of the American Chemical Society, 120, 5579. 28. html. Chapter 2 Investigation of Reaction Mechanisms by Product Studies T. W. 1 Introduction and overview – why study organic reaction mechanisms? Reaction mechanisms have been an integral part of the teaching of organic chemistry and in the planning of routes for organic syntheses for about 50 years [1].

Closely similar to those of more conventional physical organic chemistry (see Chapter 12). 11 clearly relates to the familiar Michael reaction, but the mechanism, whose elucidation is described in Chapter 12, is very different [27]. The most important feature of this reaction, of course, is the asymmetric induction which is brought about by use of a chiral ligand for the catalytically active metal centre, a recurrent and very important theme in catalysis by organometallics. 12) is more removed from conventional organic chemistry than the above Michael-like reaction, and its investigation has been a major challenge (see Chapter 12).

1). g. 2). Knowledge of reaction intermediates (see Chapter 9) is also important for mechanistic understanding and yield optimisation. 4 and Chapter 12). 4). Knowledge of minor or intermediate products is particularly helpful in designing reaction conditions to optimise the yield of a desired final product. The formation of relatively stable intermediate products can be of direct commercial significance. Details of commercial processes are not usually considered in academic texts for several reasons, including their commercial sensitivity and the financial, technical and legal complexity.

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